| 片状MoS2/MoS1.5Se0.5纳米复合材料的制备及其摩擦学性能研究 | |
| Preparation and Tribological Properties of Plate-Like MoS2/MoS1.5Se0.5 Nanocomposites | |
| 摘要: 将钼粉与升华硫和硒粉的混合粉末按一定化学计量比混合，通过固相反应法成功制备出了均匀的片状纳米颗粒。分别使用X射线粉末衍射仪(XRD)、扫描电子显微镜(SEM)以及透射电子显微镜(TEM)对该纳米粉体进行结构表征和分析，发现该粉体为MoS2/MoS1.5Se0.5混合晶相，晶粒尺寸在300~600 nm，厚度约为5 nm的片状结构。将该MoS2/MoS1.5Se0.5纳米片作为润滑油添加剂添加到基础油中，使用UMT-2型摩擦磨损试验机对其摩擦学性能进行测试，并对摩擦机理进行了解释，结果表明MoS2/MoS1.5Se0.5纳米片作为润滑油添加剂具有良好的减摩抗磨性能。 | |
| 关键词: MoS2/MoS1.5Se0.5纳米复合材料 固相法 摩擦性能 固体添加剂 | |
| 基金项目: | |
| Abstract: The plate-like nanoparticles with uniform size were synthesized by a Solid-state thermal reaction successfully between micro-sized Mo with the mixed powders of S and Se, and then studied by X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) to determine the microstructure and morphology. The result indicated that the nanoplates were composite phases of MoS2/MoS1.5Se0.5 nanoflakes with a length of 300-600 nm and thickness of 5 nm. The tribological properties of MoS2/MoS1.5Se0.5 nanoflakes were measured on UMT-2 tribo-tester and a tribological mechanism was proposed. The results show that MoS2/MoS1.5Se0.5 nanoflakes exhibit excellent properties of friction and wear as an additive of base oil. | |
| Keywords: MoS2/MoS1.5Se0.5 nanocomposites solid-state thermal reaction tribological properties solid additive | |
| 摘要点击次数: 1931 | |
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| 李文静,唐 华,罗 聪,李长生,唐国钢,梁家青,王 芬,晋 跃,李冬生.片状MoS2/MoS1.5Se0.5纳米复合材料的制备及其摩擦学性能研究[J].无机化学学报,2012,28(8):1587-1592. | |
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