MoS2纳米花的溶剂热合成及其表征 |
Flower-like MoS2 Nanoparticles: Solvothermal Synthesis and Characterization |
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摘要: |
关键词: MoS2纳米花 溶剂热合成 结构表征 |
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Abstract: Flower-like MoS2 nanoparticles have been synthesized through a mild solvothermal reaction with the aid of ethanol aqueous solution,and characterized by scanning electron microscopy(SEM),X-ray diffraction(XRD) and low temperature nitrogen adsorption-desorption. The flower is composed of the ultra-thin nanosheets of 10 nm in thickness. The influence of the reaction temperature and the reaction time on the formation of the flowers was evaluated. The optimal experimental conditions were determined as follows:the molar ratio of 1∶1 between ethanol and water,reaction temperature of 190 ℃ and reaction time of 24 h. |
Keywords: nanometer flower MoS2 solvothermal synthesis structure characterization |
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孙燕丽,王世铭,王琼生.MoS2纳米花的溶剂热合成及其表征[J].无机化学学报,2008,24(6):1003-1007. |
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