| 对氟苯甲醛水杨酰腙镍(II)配合物的合成、表征及其晶体结构 | |||||||||||||
| Synthesis, Characterization and Crystal Structure of Bis(p-fluorobenzaldehyde salicylhydrazone) Nickel(II) | |||||||||||||
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| 摘要: | |||||||||||||
| 关键词: 对氟苯甲醛水杨酰腙 镍配合物 晶体结构 合成 | |||||||||||||
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| Abstract: A nickel(II) complex Ni(C14H10N2O2F)2 was synthesized from p-fluorobenzaldehyde salicylhydrazone and Ni(CH3COO)2·4H2O and crystallized by diffusion, the structure of which was characterized by IR spectrum, 1H NMR, and X-ray single-crystal diffraction. The complex crystallizes in monoclinic space group C2/c with a=2.460 6(2) nm, b=0.774 1(1) nm, c=1.534 9(1) nm, β=122.300(1)°, and V=2.471 1(4), Z=8, Dc=1.541 g·cm-3. We reported the IR, 1H NMR, crystal structure. CCDC: 638652. | |||||||||||||
| Keywords: p-fluorobenzaldehyde salicylhydrazone nickel(II) complex crystal structure synthesis | |||||||||||||
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| 张淑萍,刘昭第,陈水生,魏影,邵思常.对氟苯甲醛水杨酰腙镍(II)配合物的合成、表征及其晶体结构[J].无机化学学报,2007,23(6):1069-1071. | |||||||||||||
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