Co-Fe普鲁士蓝类配合物纳米颗粒的微乳液法制备与表征(英文) |
Synthesis and Characterization of Cobalt-iron Prussian Blue Analogue Nanoparticles by Microemulsion |
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摘要: |
关键词: 微乳液 Triton X-100 普鲁士蓝类配合物 纳米颗粒 |
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Abstract: Highly oriented cubic, hollow cubic and spherical nanoparticles of cobalt-iron Prussian blue analogues were synthesized in poly oxyethylene tertoctylphenyl ether (TritonX-100)/n-hexanol/cyclohexane microemulsion. The effects of the water-to-surfactant molar ratio (w), the reactant concentration and the reaction temperature on the morphology of cobalt-iron Prussian blue analogues were studied. The samples were characterized by transmission electron microscopy (TEM), field emission scan electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD) and infrared spectroscopy (IR). |
Keywords: microemulsion Triton X-100 Prussian blue analogues nanoparticle |
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方建,杜贤龙,吕辉鸿,郭丹,赵继华,沈伟国.Co-Fe普鲁士蓝类配合物纳米颗粒的微乳液法制备与表征(英文)[J].无机化学学报,2007,23(5):923-927. |
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