溶胶-凝胶涂附电纺纳米纤维制备ZrO2纳米管 |
Zirconium Dioxide Nanotubes from Sol-gel Coating of Electrospun Polymer Fibers |
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摘要: |
关键词: 静电纺丝 ZrO2 纳米管 PBS |
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Abstract: Stable zirconia sol was prepared using inorganic salt(zirconia chloride octahydrate) as the precursor and H2O2 as the catalyst. ZrO2-PBS coaxial nanofibers were fabricated using the sol-gel coating technique to filling poly butylenes succinate(PBS) fibers with zirconium dioxide by electrospun. ZrO2 nanotubes were obtained via calcining ZrO2-PBS coaxial nanofibers. The ZrO2 nanotubes were characterized by TG, SEM and TEM, respectively. The results show that ZrO2 nanotubes with a diameter of 50~100 nm are obtained after calcining ZrO2-PBS coaxial nanofibers at 450 ℃. |
Keywords: electrospinning ZrO2 nanotubes PBS |
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伞振鑫,李从举,李小宁.溶胶-凝胶涂附电纺纳米纤维制备ZrO2纳米管[J].无机化学学报,2007,23(5):879-882. |
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