磷酸铵与多聚磷酸铵插层可膨胀石墨的制备 |
Preparation of Expandable Graphite Intercalated by Ammonium Phosphate and Ammonium Polyphosphate |
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摘要: |
关键词: 石墨 可膨胀石墨 磷酸铵 多聚磷酸铵 |
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Abstract: Expandable graphite intercalated by ammonium phosphate (AP) or ammonium polyphosphate (APP) was prepared by direct intercalation and two-step method, respectively. The products from two-step method show higher expansion volume, more weight increase and more weight loss after expansion, suggesting that the two-step method is a favorable method for preparation of APP intercalated EG. XRD provides convincing evidence for successful formation of APP-EG by showing strong diffraction peak at much lower 2θ angle. Scanning electron microscopy (SEM) with energy dispersive X-ray Spectroscopy (EDS) gives more evidence for intercalation of APP in the graphite layers. |
Keywords: graphite expandable graphite ammonium phosphate ammonium polyphosphate |
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韩志东,张达威,董丽敏,张显友.磷酸铵与多聚磷酸铵插层可膨胀石墨的制备[J].无机化学学报,2007,23(2):286-290. |
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