| 混配配合物[Zn(CF3COO)2(C7H6NS)2]的合成、晶体结构及表征 | |
| Synthesis, Crystal Structure and Spectral Characterization of the Complex [Zn(CF3COO)2(C7H6NS)2] | |
| 摘要: | |
| 关键词: Zn(Ⅱ)配合物 谱学表征 晶体结构 | |
| 基金项目: | |
| Abstract: A mixed complex [Zn(CF3COO)2(C7H6NS)2] was synthesized based on the reaction of Zn(CF3COO)2 and 2-aminobenzothiazol (C7H6NS) in methanol. The structure of the complex was characterized by elemental analysis, IR, 1H NMR and thermal analysis. The crystal structure of the complex was determined by X-ray single crystal diffraction. The crystal belongs to monoclinic system with space group C2/c, a=3.174 3(9) nm, b=1.010 0(3) nm, c=1.723 1(5) nm, β=118.841(4)°, V=4.839(2) nm3; Dc=1.625 g·cm-3; Z=8; F(000)=2 368; μ=1.266 mm-1. CCDC: 600233. | |
| Keywords: Zn(Ⅱ) complex spectral characterization crystal structure | |
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| 马卫兴,钱保华,李善忠,王建,许兴友,陆路德,宋海斌.混配配合物[Zn(CF3COO)2(C7H6NS)2]的合成、晶体结构及表征[J].无机化学学报,2006,22(10):1925-1928. | |
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