熔盐法合成NiO纳米微晶
Synthesis of NiO Nano-crystal Powders by Molten Salt Method
作者单位
王健 清华大学化学系北京 100084 
邓小芝 清华大学化学系北京 100084 
邱新平 清华大学化学系北京 100084 
朱文涛 清华大学化学系北京 100084 
武增华 清华大学化学系北京 100084 
摘要: 
关键词: 氧化镍  纳米晶  熔盐法  弱团聚
基金项目: 
Abstract: NiO nano-crystal powders with cubic structure were synthesized by molten salt method. The synthesized materials were characterized by XRD, TEM, N2 adsorption-desorption and TG, etc. Not only are the eminent characters of weak agglomeration, narrow distribution and fine crystalline configuration, but the average crystal sizes of synthesized NiO powders could be efficiently controlled from 10 nm to 100 nm by changing the calcination conditions, such as calcination temperature, calcination time, and proportion of molten salt KNO3. Molten salt method is technologically easy and cheap, for the production of NiO nano-crystal powders in industrial scale.
Keywords: NiO  nano-crystal  molten salt method  weak agglomeration
 
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王健,邓小芝,邱新平,朱文涛,武增华.熔盐法合成NiO纳米微晶[J].无机化学学报,2006,22(10):1874-1878.
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