草酸盐共沉淀法制备Y1.84La0.16O3纳米粉体 |
Preparation of Y1.84La0.16O3 Nanopowders by Oxalate Co-precipitation Method |
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关键词: Y1.84La0.16O3 纳米粉体 草酸盐共沉淀法 透明陶瓷 |
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Abstract: Nanopowder of Y1.84La0.16O3 was prepared by oxalate co-precipitation method. The powder was characterized by TG-DTA, XRD and TEM. The results show that the precursor is Re2(NO3)2(C2O4)2·2H2O (Re=Y, La), and the Y1.84La0.16O3 nanopowders produced by calcining the precursor at 1 000 ℃ for 4 h are 20~40 nm spherical particles and well dispersed. The powders were with high sintering activity and could be fabricated to transparent ceramic without additive at 1 450~1 550 ℃ in H2 atmosphere for 3 hours. The total transmission of the transparent ceramic could reach 80%. |
Keywords: Y1.84La0.16O3 nanopowder oxalate co-precipitation method transparent ceramic |
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唐在峰,丁君,杨秋红,徐军.草酸盐共沉淀法制备Y1.84La0.16O3纳米粉体[J].无机化学学报,2006,22(10):1871-1873. |
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