水热法制备具有光滑表面的球形Y2O3∶Eu3+发光材料(英文) |
Hydrothermal Synthesis of Spherical Y2O3∶Eu3+ Luminescent Materials with Smooth Surface |
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摘要: |
关键词: 球形Y2O3∶Eu3+ 荧光粉 水热法 发光材料 |
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Abstract: The spherical Y2O3∶Eu3+ luminescent particles with size of 0.5~3 μm and smooth surface were synthesized by hydrothermal method. The resulted Y2O3∶Eu3+ precursors and the calcined particles were characterized by differential thermal analysis (DTA) and thermogravimetric (TG) analysis, X-ray diffraction (XRD), Fourier-transform IR spectroscopy (FTIR), scanning electron microscopy (SEM) and photoluminescence spectra (PL). FTIR, TG-DTA, XRD measurements show that the precursors are crystal with hydroxyl and carbonate group, and the pure cubic yttria is obtained after annealing above 700 ℃. The SEM images indicate that the Y2O3∶Eu3+ particles are in spherical shape and with smooth surface. PL analysis shows that the particles present characteristic red emission of Eu3+. |
Keywords: spherical Y2O3∶Eu3+ phosphors hydrothermal method luminescent materials |
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刘桂霞,洪广言,王进贤,董相廷.水热法制备具有光滑表面的球形Y2O3∶Eu3+发光材料(英文)[J].无机化学学报,2006,22(8):1535-1539. |
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