无溶剂热分解单源前驱体法制备有机单分子层表面修饰NiS纳米微粒
Solventless Synthesis of Monolayer Protected NiS Nanoparticles from Nickel Hexadecylxanthate Single-Source Precursor by a Thermolytic Method
作者单位
张春丽 河南大学特种功能材料重点实验室开封 475001 
张晟卯 河南大学特种功能材料重点实验室开封 475001 
卢春 河南大学特种功能材料重点实验室开封 475001 
吴志申 河南大学特种功能材料重点实验室开封 475001 
张平余 河南大学特种功能材料重点实验室开封 475001 
摘要: 
关键词: 纳米颗粒  无溶剂合成  单源前驱体  NiS
基金项目: 
Abstract: NiS Nanoparticles were synthesized from nickel hexadecylxanthate single-source precursor via a thermolytic method. The partial xanthate ligand dissociated from precursor absorbed to the surface of NiS nanoparticles as capping agent. The products were characterized by FTIR,XRD and TEM. The results indicate that NiS nanoparticles have excellent dispersibility with hexagonal structure and the average diameter is 15 nm.
Keywords: nanoparticles  solventless synthesis  single-source precursor  thermolytic method
 
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张春丽,张晟卯,卢春,吴志申,张平余.无溶剂热分解单源前驱体法制备有机单分子层表面修饰NiS纳米微粒[J].无机化学学报,2006,22(3):581-584.
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