水热法合成K0.5Bi0.5TiO3纳米陶瓷粉体 |
Hydrothermal Synthesis of K0.5Bi0.5TiO3 Lead-free Piezoelectric Ceramic |
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摘要: |
关键词: 水热法 钛酸铋钾 无铅压电陶瓷 |
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Abstract: K0.5Bi0.5TiO3(KBT)nanocrystalline particles were hydrothermally synthesized from Bi(NO3)3·5H2O, TiO2 and KOH. The crystal phase, chemical composition and microstructure were characterized by XRD, XRF, Raman scattering spectroscopy and TEM. The results indicated that the products were pure perovskite structured K0.5Bi0.5TiO3 with chemical stoichiometry and perovskite structure. The TEM observation revealed that the particles possessed a feature of cubic shape and a nano-scale of about 40 nm. The KBT ceramics sintered at 1 040 ℃ from hydrothermal powders show higher density and better electric properties than that prepared by a solid-state reaction method. |
Keywords: hydrothermal method K0.5Bi0.5TiO3 lead-free piezoelectric ceramic |
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摘要点击次数: 1439 |
全文下载次数: 2016 |
侯磊,侯育冬,宋雪梅,朱满康,汪浩,严辉.水热法合成K0.5Bi0.5TiO3纳米陶瓷粉体[J].无机化学学报,2006,22(3):563-566. |
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