沸腾回流法制备纳米NiZn铁氧体的研究
Nanometer NiZn Ferrite Prepared by Refluxing Method
作者单位
钟海胜 清华大学化学系北京 100084 
李强 清华大学化学系北京 100084 
张一玲 清华大学材料科学与工程系北京 100084 
钟志锋 清华大学化学系北京 100084 
张阳 清华大学化学系北京 100084 
摘要: 
关键词: 沸腾回流法  NiZn铁氧体  尖晶石相
基金项目: 
Abstract: Nanometer NiZn ferrite powder with spinel structure was prepared by a new chemical method —— refluxing method. Refluxing time and pH value of coprecipitation were discussed based on the XRD analysis and pH value measurement. The optimum refluxing time and pH value of coprecititation were 6 hours and 9.5~11.0, respectively. Ni0.5Zn0.5Fe2O4 powder prepared by refluxing method was about 20 nm by TEM analysis. And VSM results revealed that the prepared Ni0.5Zn0.5Fe2O4 powder had typical soft magnetic characteristics.
Keywords: refluxing method  NiZn ferrite  spinel phase
 
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钟海胜,李强,张一玲,钟志锋,张阳.沸腾回流法制备纳米NiZn铁氧体的研究[J].无机化学学报,2006,22(2):375-378.
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