反相微乳液法合成纳米钛酸钡球形颗粒 |
Preparation of BaTiO3 Spherical Nanoparticles by Reverse Microemulsion |
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关键词: W/O微乳液 球形粒子 钛酸钡 纳米颗粒 |
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Abstract: Nanosized BaTiO3 spherical particles were synthesized in reverse microemulsion consisting of water, Triton-10, n-hexanol and cyclohexane. The reaction conditions were optimized on the basis of the study of the influence of the molar ratio of water to surfactant, the concentration of reactants and ageing time on the shape and size of BaTiO3 particles. The prepared BaTiO3 samples were characterized by TEM and XRD. The results show that the spherical BaTiO3 nanoparticles with an average size of 20~80 nm belong to single tetragonal system. The molar ratio of barium to titanium of products is 1.0 from ICP analysis. |
Keywords: W/O microemulsion spherical particle barium titanate nanoparticle |
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宋方平,朱启安,王树峰,陈万平.反相微乳液法合成纳米钛酸钡球形颗粒[J].无机化学学报,2006,22(2):355-358. |
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