| 大环草酰胺配合物CuC33H28Cl2N4O3的合成和晶体结构(英) |
| Synthesis and Crystal Structure of Macrocyclic Oxamide Complex CuC33H28Cl2N4O3 |
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| 摘要: |
| 关键词: 大环草酰胺配合物 晶体结构 光谱表征 |
| 基金项目: |
| Abstract: A novel macrocyclic oxamide complex CuL (L=C33H28Cl2N4O3) has been synthesized and characterized by elemental analysis, IR spectrum, UV-Visible spectrum and single crystal X-ray diffraction. It crystallizes in the monoclinic system, space group P21/n. The lattice parameters are: a=0.848 8(3) nm, b=1.904 9(7) nm, c=1.868 1(7) nm, β=92.794 (6)° and V=3.016 8(19) nm3, Z=4. The results show that the coordination geometry around copper(Ⅱ) in the complex is aberrant tetragonal-plane. CCDC: 265601. |
| Keywords: macrocyclic oxamide complex crystal structure spectroscopic characterization |
| 投稿时间：2005-03-28 修订日期：2005-09-12 |
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| 周旭光,孙亚秋,王庆伦,杨光明,廖代正.大环草酰胺配合物CuC33H28Cl2N4O3的合成和晶体结构(英)[J].无机化学学报,2005,21(12):1853-1856. |
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