高分散纳米二氧化钛混合晶体的合成、结构与光催化性能 |
Synthesis, Structure and Photocatalysis of Nano-TiO2 Mixed Crystals |
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摘要: |
关键词: 高分散纳米二氧化钛 混晶 制备 光催化性能 |
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Abstract: Using TiCl4 and urea as the raw materials and nanometric carbon black as plate, nanometric mix-crystals of rutile and anatase TiO2 were prepared at 100 ℃ for 10~180 min by homogeneous precipitation method. The effects of pH on the ratio of nanometer TiO2 mix-crystals were also discussed. TEM measurement indicates that the TiO2 is spherical particles, and the average diameter of the particles is 20 nm. XRD and TG-DTA were also used to characterize the nanometer mix-crystal materials. The photocatalytic experiment show that the mix-crystal material has the best photocatalytic reactivity. After being irradiated under the sunlight for 40 min, the compound can completely degrade the acid-red 3R. |
Keywords: nano-TiO2 mix-crystal preparation photocatalys |
投稿时间:2004-08-23 修订日期:2004-10-19 |
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王振兴,丁士文,张美红.高分散纳米二氧化钛混合晶体的合成、结构与光催化性能[J].无机化学学报,2005,21(3):437-440. |
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