无氨湿法制备纳米晶In2O3及表征
Preparation and Characterization of Nanometer Indium Oxide by Precipitation Method without Ammonia Water
作者单位
刘兴芝 辽宁大学化学科学与工程学院稀散元素化学研究所沈阳 110036 
司 伟 辽宁大学化学科学与工程学院稀散元素化学研究所沈阳 110036 
丁 超 辽宁大学化学科学与工程学院稀散元素化学研究所沈阳 110036 
王鲁宁 辽宁大学化学科学与工程学院稀散元素化学研究所沈阳 110036 
臧树良 辽宁大学化学科学与工程学院稀散元素化学研究所沈阳 110036 
摘要: 
关键词: 超声波 均匀沉淀法 纳米晶In2O3
基金项目: 
Abstract: Preparation of In2O3nano-scale powders by ultrasonic and homogeneous precipitation, using metal In and urea as raw materials, was reported for the first time, while the effects of reaction temperature, the ratio of the materials and the pH etc. on the preparation was dicussed. This method can be operated and industrialized easily with very low cost. The structural properties of precursor and In2O3were characterized by TG-DTA, XRD, ESCA and TEM. The results show that In2O3produced are very pure, monophase and spherical nano-scale powders with average size of 25 nm.
Keywords: ultrasonic homogeneous precipitation nanometersized In2O3
 
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刘兴芝,司 伟,丁 超,王鲁宁,臧树良.无氨湿法制备纳米晶In2O3及表征[J].无机化学学报,2004,20(8):975-979.
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