| 两种一维纳米结构钒氧化物的合成与表征 |
| Syntheses and Characterizations of Two Kinds of One-dimensional Nanostructure Vanadium Oxide |
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| 摘要: 在水热条件下，分别利用十六胺和十六烷基三甲基溴化铵为模板，合成了两种一维纳米结构的钒氧化物：纳米管和纳米棒，采用XRD、TEM、HRTEM、FT-IR、TG/DTA对产物的形貌和结构进行了表征。研究表明，纳米管的长度主要分布在1～10 μm，外径50～100 nm，内径10～30 nm；纳米棒长1～2 μm，径向尺寸50～200 nm。 |
| 关键词: 钒氧化物 纳米管 纳米棒 合成 表征 |
| 基金项目: |
| Abstract: Syntheses of vanadium oxide nanotubes and vanadium dioxide nanorods were carried out successfully using hexadecylamine and cetyltrimethylammonium bromide as structure-directing template respectively in hydrothermal condition. Morphologies and structures of the samples were characterized by XRD, TEM, HRTEM, FT-IR and TG/DTA. Vanadium oxide nanotubes have outer diameters from 30～100 nm and inner diameters from 10～30 nm with length up to several micrometers. Vanadium dioxide nanorods are always 1～2 μm in length and have a diameter between 50～100 nm. The first time vanadium dioxide nanorods were obtained via an ammonium template-assisted hydrothermal method. |
| Keywords: vanadium oxide nanotubes nanorods synthesis characterization |
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| 陈 文,彭俊锋,麦立强,徐 庆,朱泉峣.两种一维纳米结构钒氧化物的合成与表征[J].无机化学学报,2004,20(2):147-151. |
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