TiSe2纳米管的制备和表征
Preparation and Characterization of TiSe2 Nanotubes
作者单位
陶占良 南开大学新能源材料化学研究所,天津,300071 
李锁龙 南开大学新能源材料化学研究所,天津,300071 
范晓彬 南开大学新能源材料化学研究所,天津,300071 
陈 军 南开大学新能源材料化学研究所,天津,300071 
摘要: 
关键词: 二硒化钛 纳米管 固相反应
基金项目: 
Abstract: The ball-milled mixture of Ti and Se powders was carried out a solid-phase reaction at 600℃.The asprepared sample had been characterized by X-ray diffraction(XRD),scanning electron microscopy(SEM),transmission electron microscopy(TEM)and high-resolution transmission electron microscopy(HRT EM).The result shows that the products are multiwalled TiSe2 nanotubes with open-ended tips,which are about 15nm in outer diameter,several micron in lengths,and 0.6nm of interlayer spacing.
Keywords: titanium s elenide nanotube solid-phase reaction
 
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陶占良,李锁龙,范晓彬,陈 军.TiSe2纳米管的制备和表征[J].无机化学学报,2004,20(1):99-101.
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