单壁纳米碳管的纯化研究(英文) | |
Study on Purification of Single-Walled Carbon Nanotubes | |
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关键词: 单壁纳米碳管 拉曼光谱 热重分析 | |
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Abstract: A purification method to remove the metal catalysts and impurity carbon materials from arc-discharge-grown single-walled carbon nanotubes (SWCNTs) has been developed. Microporous membrane and the oxidation in the air for the crude SWCNTs were used to eliminate the coexisting metal catalysts nanoparticles,carbon nanoparticles and amorphous carbon. Then we used the high resolution transmission electron microscopy (HRTEM) to characterize the crude SWCNTs prepared by arc-discharge method and the purified SWCNTs. The Raman spectra and the thermogravimetric analysis (TGA) were also utilized to analyze the approach of our purification for SWCNTs. With this method the SWCNTs with the purity more than 95% could be obtained. | |
Keywords: single-walled carbon nanotube(SWCNTs) Raman spectra thermogravimetric analysis(TGA) | |
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王新庆,王淼,李振华,朱海滨,王凤飞,卢焕明,何丕模.单壁纳米碳管的纯化研究(英文)[J].无机化学学报,2003,19(6):594-598. | |
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