LiMn2O4的湿法合成及锰的光度法测定研究 |
Synthesis of LiMn2O4 Spinel with Solution Method and Spectrophotometric Determination of Mn |
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摘要: |
关键词: LiMn2O4尖晶石 湿法 光度法 锰测定 |
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Abstract: The LiMn2O4 spinel was prepared by wet method using Li2CO3, Mn(CH3COO)2·4H2O and CO2 as raw ma-terials. The products were measured by TG/DTA, XRD, IR. The results Showed that the sample calcined at 800℃ for 10h was well crystallized monophase product. The contents of Mn(Ⅲ) and Mn(Ⅳ) of LiMn2O4 spinel were determined simultaneously by spectrophotometric analysis with pyrophosphoric acid. |
Keywords: LiMn2O4 spinel wet method spectrophotometric analysis Mn determination |
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余鼎,赖琼钰,卢集政,韦勇强,吉晓洋,杨争.LiMn2O4的湿法合成及锰的光度法测定研究[J].无机化学学报,2003,19(5):552-556. |
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