LiMn2O4的湿法合成及锰的光度法测定研究
Synthesis of LiMn2O4 Spinel with Solution Method and Spectrophotometric Determination of Mn
作者单位
余鼎 四川大学化学学院成都 610064 
赖琼钰 四川大学化学学院成都 610064 
卢集政 四川大学化学学院成都 610064 
韦勇强 四川大学化学学院成都 610064 
吉晓洋 四川大学分析测试中心成都 610064 
杨争 四川大学分析测试中心成都 610064 
摘要: 
关键词: LiMn2O4尖晶石 湿法 光度法 锰测定
基金项目: 
Abstract: The LiMn2O4 spinel was prepared by wet method using Li2CO3, Mn(CH3COO)2·4H2O and CO2 as raw ma-terials. The products were measured by TG/DTA, XRD, IR. The results Showed that the sample calcined at 800℃ for 10h was well crystallized monophase product. The contents of Mn(Ⅲ) and Mn(Ⅳ) of LiMn2O4 spinel were determined simultaneously by spectrophotometric analysis with pyrophosphoric acid.
Keywords: LiMn2O4 spinel wet method spectrophotometric analysis Mn determination
 
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余鼎,赖琼钰,卢集政,韦勇强,吉晓洋,杨争.LiMn2O4的湿法合成及锰的光度法测定研究[J].无机化学学报,2003,19(5):552-556.
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