| 溶剂热/水热条件下空旷结构草酸锌的合成 |
| Zinc Oxalates with Open Frameworks Synthesized by Solvothermal/Hydrothermal Methods |
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| 摘要: 应用水热法及溶剂热方法，选择两种模板剂1，2-丙二胺和4，5-二氮芴-9-酮连氮(L)设计合成了草酸锌空旷结构材料[Zn2(C2O4)3][C3H12N2]·H2O (Ⅰ)和[Zn2(C2O4)3]·L·6[H3O] (Ⅱ)，使用CHN元素分析、 |
| 关键词: 草酸锌 空旷结构 水热 溶剂热 |
| 基金项目: |
| Abstract: Two kinds of novel open frameworks zinc oxalates， [Zn2(C2O4)3][C3H12N2]·H2O(Ⅰ) and Zn2(C2O4)3]·L·6[H3O] (Ⅱ)， have been synthesized by solvothermal or hydrothermal methods in the presences of different kinds of amines，C3H9N2 and 4，5-diazafluren-9-one-N2.The composites and structures were conformed by elemental analy-ses， XRD， IR， SEM， and TG/DSC， etc. |
| Keywords: zinc oxalates open frameworks hydrothermal solvothermal |
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| 胡娟,高秋明.溶剂热/水热条件下空旷结构草酸锌的合成[J].无机化学学报,2003,19(1):64-68. |
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