| [Ni(dien)2]2[Mn(NCS)6]·H2O的合成、晶体结构 | |||||||||||
| Synthesis and Crystal Structure of [Ni(dien)2]2[Mn(NCS)6]·H2O | |||||||||||
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| 关键词: 硫氰酸根 二乙烯三胺 多核配合物 晶体结构 | |||||||||||
| 基金项目: | |||||||||||
| Abstract: The crystal of [Ni(dien)2]2[Mn(NCS)6]·H2O was synthesized and the structure of its single crystal was determined by X-ray diffraction. The crystal is monoclinic system, space group P21/c with a=16.544(3),b=15.137(2), c=17.334(3)?, β=99.90(1)°, V=4276.3(12)?3, Z=4, Dc=1.479g·cm-3, Mr=951.55, F(000)=1998, μ=1.489mm-1, R=0.0399, Rw=0.0958. IR was also determined. | |||||||||||
| Keywords: thiocyanate diethylenetriamine polynuclear complex crystal structure | |||||||||||
| 摘要点击次数: 1438 | |||||||||||
| 全文下载次数: 1659 | |||||||||||
| 沈良,徐迅,徐端钧,徐元植.[Ni(dien)2]2[Mn(NCS)6]·H2O的合成、晶体结构[J].无机化学学报,2002,18(3):309-312. | |||||||||||
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