高温气相合成纳米TiO2-Al2O3复合颗粒的形态 |
Morphology of High Temperature Vapor-Phase Synthesized Nanophase TiO2-Al2O3 Composite Particles |
|
摘要: |
关键词: 纳米颗粒 气相反应 功能陶瓷 |
基金项目: 国家计委九五攻关项目(No.9655402);国家自然科学基金(No.29506045) |
Abstract: Nanophase TiO2-Al2O3 composite particles synthesized by gas phase oxidation of TiCl4 and AlCl3 in an aerosol reactor were characterized by EDS, XPS, TG-DTA, TEM, XRD and BET surface area analysis. The results showed that the morphological structure of the composite particles were influenced by AlCl3 feed ratio and reaction temperature. When Xinlet=2.80 and T=1400℃, the composite particles were mainly composed of rutile TiO2,α Al2O3, and Al2TiO5, the average particle size was 25.3 nm and GSD (Geometric tandaed Squace Deviation) was 1.51. Other processing parameters affecting the particle size was also analyzed. |
Keywords: nanophase particles vapor-phase reaction functional ceramic |
投稿时间:1999-10-18 修订日期:2000-01-24 |
摘要点击次数: 1595 |
全文下载次数: 2436 |
施利毅,李春忠,房鼎业,古宏晨,朱以华,陈爱平.高温气相合成纳米TiO2-Al2O3复合颗粒的形态[J].无机化学学报,2000,16(4):683-687. |
查看全文 查看/发表评论 下载PDF阅读器 |
Support information: |
|
|
|