MCM-41分子筛的合成及129Xe核磁共振的研究 |
Sythesis of the Mesoporous Molecular Sieve MCM-41 and 129Xe NMR Studies |
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摘要: |
关键词: MCM-41中孔分子筛 129Xe核磁共振 |
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Abstract: Purely siliceous MCM-41 with a narrow pore-size distribution, different pore size, high surface area was synthesized . As prepared, calcined and catalytically tested MCM-41 materials have been comprehensively characterized by N2 adsorption/desorption at 77K and 129Xe NMR. By adding mesitylene during the synthesis, the pore size of MCM-41 was enlarged to 5.2nm. The chemical shift in 129Xe NMR spectroscopy of adsorbed xenon indicates that the MCM-41 is one dimensional pore channels . |
Keywords: MCM-41 mesporous material 129Xe NMR |
投稿时间:1999-03-30 修订日期:1999-09-22 |
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孙克宁,曹莹,邵延斌.MCM-41分子筛的合成及129Xe核磁共振的研究[J].无机化学学报,2000,16(1):115-118. |
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