MCM-41分子筛的合成及129Xe核磁共振的研究
Sythesis of the Mesoporous Molecular Sieve MCM-41 and 129Xe NMR Studies
作者单位
孙克宁 哈尔滨工业大学, 哈尔滨150001 
曹莹 哈尔滨工业大学, 哈尔滨150001 
邵延斌 哈尔滨工业大学, 哈尔滨150001 
摘要: 
关键词: MCM-41中孔分子筛  129Xe核磁共振
基金项目: 
Abstract: Purely siliceous MCM-41 with a narrow pore-size distribution, different pore size, high surface area was synthesized . As prepared, calcined and catalytically tested MCM-41 materials have been comprehensively characterized by N2 adsorption/desorption at 77K and 129Xe NMR. By adding mesitylene during the synthesis, the pore size of MCM-41 was enlarged to 5.2nm. The chemical shift in 129Xe NMR spectroscopy of adsorbed xenon indicates that the MCM-41 is one dimensional pore channels .
Keywords: MCM-41 mesporous material  129Xe NMR
投稿时间:1999-03-30 修订日期:1999-09-22
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孙克宁,曹莹,邵延斌.MCM-41分子筛的合成及129Xe核磁共振的研究[J].无机化学学报,2000,16(1):115-118.
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