水热法合成MCM-41分子筛时添加辅助烃的影响 |
SYNTHESIS MESOPOROUS MOLECULAR SIEVE MCM-41 IN THE SYSTEM AUXILIARY ALKANES Na2O-Al2O3-SiO2-CTAB-H2O AND THEIR PROPERTIES |
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摘要: |
关键词: MCM-41 水热合成 辅助烃 表征 |
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Abstract: By using cetyltrimethylammonium bromite (CTAB) as template, influences of auxiliary alkanes (n-hexane, n-heptane, iso-octane, and petroleum ether) for synthesizing mesoprours molecular sieve MCM-41 with more than 4 nm pore have studied in hydrothermal system. It was proved by experiments that molecular sieve MCM-41 with d100>4 nm could be obtained with putting auxiliary alkanes. As-synthesized samples have been characterized by XRD, SEM and N2 adsorption. The experimental results showed that adding auxiliary alkanes made decreasing order of molecular sieve MCM-41. |
Keywords: molecular sieve MCM-41 synthesis auxiliary alkanes characterization |
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董晋湘,徐红,刘光焕,高振起,吴锋.水热法合成MCM-41分子筛时添加辅助烃的影响[J].无机化学学报,1999,15(1):104-109. |
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