非酸性介质中SAPO-5、SAPO-34型分子筛的合成 |
SYNTHESES OF MOLECULAR SIEVES SAPO-5 AND SAPO-34 IN NON-ACID MEDIUM |
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摘要: 以三乙胺为模板剂,用水热晶化法,首次在非酸性介质中合成了SAPO-5、SAPO-34型分子筛.通过X-射线粒未衍射、电子探针微区分析、电子能谱及红外光谱进行了结构研究,确认合成样品为SAPO-5和SAPO-34型分子筛,并对它们的化学组成、热稳定性、表面酸性及吸附性能进行了研究。 |
关键词: 分子筛 磷酸硅铝 三乙胺 非酸性介质 |
基金项目: |
Abstract: The molecular sieves SAPO-5 and SAPO-34 have been synthesized hydrothermally in the presence of triethylamine templates in non-acid medium. The determination X-ray diffraction, electron scanning microscope, X-ray photoelectron spectroscopy, infrared spectrum showed the difference of the two kinds of silicoaluminophosphate molecular sieves. Some properties, including thermal stability, surface acidity and adsorption property, have been studied. |
Keywords: molecular sieve silicoaluminophosphate triethylamine non-acid medium |
投稿时间:1988-01-22 |
摘要点击次数: 1801 |
全文下载次数: 1967 |
孟长功,周凤歧,孟宪平,庞文琴.非酸性介质中SAPO-5、SAPO-34型分子筛的合成[J].无机化学学报,1990,6(2):176-180. |
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